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Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia

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2019
502.pdf (404.6Kb)
Authors
Pantović-Spajić, Katarina
Sakan, S.
Đorđević, D.
Šoštarić, Tatjana
Lopičić, Zorica
Janićijević, A.
Stojanović, Ksenija
Article (Published version)
Metadata
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Abstract
The purpose of this paper was to investigate the effectiveness of three different extraction agents for the extraction of 25 elements from sediment samples collected from 4 artificial lakes and 12 rivers in Serbia (33 samples in total). The extraction efficiency of the agents was evaluated by its ability to extract the highest quantity of the elements. For that purpose, three acids (1M HCl, 2M HNO3 and 0.43M CH3COOH) have been used. Inductively coupled plasma atomic emission spectrometry (ICP-OES) was used for quantitative determination of following elements: Al, As, B, Ba, Be, Bi, Ca, Cd, Cr, Co, Cu, Fe, Hg, K, Li, Mg, Mn, Ni, Na, Pb, Sb, Se, Sr, V, and Zn. The extraction with 1M HCl has shown the best results for the majority of investigated elements (especially Sr, Mn and Ca). Antimony (Sb) was detected only after extraction with 0.43M CH3COOOH, while selenium (Se) could not be detected when 2M HNO3 was applied as extraction agents. The present study could be very useful for choosin...g a suitable method for specific elements and also can be helpful in the evaluation of the contaminants in freshwater sediments in Serbia. This might contribute to environmental risk assessment of the present elements.

Keywords:
River / Metals / Lake sediments / Extraction agents
Source:
Acta Periodica Technologica, 2019, 50, 189-196
Publisher:
  • Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad
Funding / projects:
  • The study of physicochemical and biochemical processes in living environment that have impacts on pollution and the investigation of possibilities for minimizing the consequences (RS-172001)
  • Developing technological processes for nonstandard copper concentrates processing with the aim to decrease pollutants emission (RS-34023)

DOI: 10.2298/APT1950189P

ISSN: 1450-7188

Scopus: 2-s2.0-85078890730
[ Google Scholar ]
1
URI
https://ritnms.itnms.ac.rs/handle/123456789/505
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Institut za tehnologiju nuklearnih i drugih mineralnih sirovina
TY  - JOUR
AU  - Pantović-Spajić, Katarina
AU  - Sakan, S.
AU  - Đorđević, D.
AU  - Šoštarić, Tatjana
AU  - Lopičić, Zorica
AU  - Janićijević, A.
AU  - Stojanović, Ksenija
PY  - 2019
UR  - https://ritnms.itnms.ac.rs/handle/123456789/505
AB  - The purpose of this paper was to investigate the effectiveness of three different extraction agents for the extraction of 25 elements from sediment samples collected from 4 artificial lakes and 12 rivers in Serbia (33 samples in total). The extraction efficiency of the agents was evaluated by its ability to extract the highest quantity of the elements. For that purpose, three acids (1M HCl, 2M HNO3 and 0.43M CH3COOH) have been used. Inductively coupled plasma atomic emission spectrometry (ICP-OES) was used for quantitative determination of following elements: Al, As, B, Ba, Be, Bi, Ca, Cd, Cr, Co, Cu, Fe, Hg, K, Li, Mg, Mn, Ni, Na, Pb, Sb, Se, Sr, V, and Zn. The extraction with 1M HCl has shown the best results for the majority of investigated elements (especially Sr, Mn and Ca). Antimony (Sb) was detected only after extraction with 0.43M CH3COOOH, while selenium (Se) could not be detected when 2M HNO3 was applied as extraction agents. The present study could be very useful for choosing a suitable method for specific elements and also can be helpful in the evaluation of the contaminants in freshwater sediments in Serbia. This might contribute to environmental risk assessment of the present elements.
PB  - Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad
T2  - Acta Periodica Technologica
T1  - Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia
EP  - 196
SP  - 189
VL  - 50
DO  - 10.2298/APT1950189P
UR  - conv_1023
ER  - 
@article{
author = "Pantović-Spajić, Katarina and Sakan, S. and Đorđević, D. and Šoštarić, Tatjana and Lopičić, Zorica and Janićijević, A. and Stojanović, Ksenija",
year = "2019",
abstract = "The purpose of this paper was to investigate the effectiveness of three different extraction agents for the extraction of 25 elements from sediment samples collected from 4 artificial lakes and 12 rivers in Serbia (33 samples in total). The extraction efficiency of the agents was evaluated by its ability to extract the highest quantity of the elements. For that purpose, three acids (1M HCl, 2M HNO3 and 0.43M CH3COOH) have been used. Inductively coupled plasma atomic emission spectrometry (ICP-OES) was used for quantitative determination of following elements: Al, As, B, Ba, Be, Bi, Ca, Cd, Cr, Co, Cu, Fe, Hg, K, Li, Mg, Mn, Ni, Na, Pb, Sb, Se, Sr, V, and Zn. The extraction with 1M HCl has shown the best results for the majority of investigated elements (especially Sr, Mn and Ca). Antimony (Sb) was detected only after extraction with 0.43M CH3COOOH, while selenium (Se) could not be detected when 2M HNO3 was applied as extraction agents. The present study could be very useful for choosing a suitable method for specific elements and also can be helpful in the evaluation of the contaminants in freshwater sediments in Serbia. This might contribute to environmental risk assessment of the present elements.",
publisher = "Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad",
journal = "Acta Periodica Technologica",
title = "Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia",
pages = "196-189",
volume = "50",
doi = "10.2298/APT1950189P",
url = "conv_1023"
}
Pantović-Spajić, K., Sakan, S., Đorđević, D., Šoštarić, T., Lopičić, Z., Janićijević, A.,& Stojanović, K.. (2019). Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia. in Acta Periodica Technologica
Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad., 50, 189-196.
https://doi.org/10.2298/APT1950189P
conv_1023
Pantović-Spajić K, Sakan S, Đorđević D, Šoštarić T, Lopičić Z, Janićijević A, Stojanović K. Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia. in Acta Periodica Technologica. 2019;50:189-196.
doi:10.2298/APT1950189P
conv_1023 .
Pantović-Spajić, Katarina, Sakan, S., Đorđević, D., Šoštarić, Tatjana, Lopičić, Zorica, Janićijević, A., Stojanović, Ksenija, "Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia" in Acta Periodica Technologica, 50 (2019):189-196,
https://doi.org/10.2298/APT1950189P .,
conv_1023 .

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