Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia

2019
Authors
Pantović-Spajić, Katarina
Sakan, S.
Đorđević, D.
Šoštarić, Tatjana

Lopičić, Zorica

Janićijević, A.
Stojanović, Ksenija

Article (Published version)
Metadata
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The purpose of this paper was to investigate the effectiveness of three different extraction agents for the extraction of 25 elements from sediment samples collected from 4 artificial lakes and 12 rivers in Serbia (33 samples in total). The extraction efficiency of the agents was evaluated by its ability to extract the highest quantity of the elements. For that purpose, three acids (1M HCl, 2M HNO3 and 0.43M CH3COOH) have been used. Inductively coupled plasma atomic emission spectrometry (ICP-OES) was used for quantitative determination of following elements: Al, As, B, Ba, Be, Bi, Ca, Cd, Cr, Co, Cu, Fe, Hg, K, Li, Mg, Mn, Ni, Na, Pb, Sb, Se, Sr, V, and Zn. The extraction with 1M HCl has shown the best results for the majority of investigated elements (especially Sr, Mn and Ca). Antimony (Sb) was detected only after extraction with 0.43M CH3COOOH, while selenium (Se) could not be detected when 2M HNO3 was applied as extraction agents. The present study could be very useful for choosin...g a suitable method for specific elements and also can be helpful in the evaluation of the contaminants in freshwater sediments in Serbia. This might contribute to environmental risk assessment of the present elements.
Keywords:
River / Metals / Lake sediments / Extraction agentsSource:
Acta Periodica Technologica, 2019, 50, 189-196Publisher:
- Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad
Funding / projects:
- The study of physicochemical and biochemical processes in living environment that have impacts on pollution and the investigation of possibilities for minimizing the consequences (RS-172001)
- Developing technological processes for nonstandard copper concentrates processing with the aim to decrease pollutants emission (RS-34023)
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Institution/Community
Institut za tehnologiju nuklearnih i drugih mineralnih sirovinaTY - JOUR AU - Pantović-Spajić, Katarina AU - Sakan, S. AU - Đorđević, D. AU - Šoštarić, Tatjana AU - Lopičić, Zorica AU - Janićijević, A. AU - Stojanović, Ksenija PY - 2019 UR - https://ritnms.itnms.ac.rs/handle/123456789/505 AB - The purpose of this paper was to investigate the effectiveness of three different extraction agents for the extraction of 25 elements from sediment samples collected from 4 artificial lakes and 12 rivers in Serbia (33 samples in total). The extraction efficiency of the agents was evaluated by its ability to extract the highest quantity of the elements. For that purpose, three acids (1M HCl, 2M HNO3 and 0.43M CH3COOH) have been used. Inductively coupled plasma atomic emission spectrometry (ICP-OES) was used for quantitative determination of following elements: Al, As, B, Ba, Be, Bi, Ca, Cd, Cr, Co, Cu, Fe, Hg, K, Li, Mg, Mn, Ni, Na, Pb, Sb, Se, Sr, V, and Zn. The extraction with 1M HCl has shown the best results for the majority of investigated elements (especially Sr, Mn and Ca). Antimony (Sb) was detected only after extraction with 0.43M CH3COOOH, while selenium (Se) could not be detected when 2M HNO3 was applied as extraction agents. The present study could be very useful for choosing a suitable method for specific elements and also can be helpful in the evaluation of the contaminants in freshwater sediments in Serbia. This might contribute to environmental risk assessment of the present elements. PB - Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad T2 - Acta Periodica Technologica T1 - Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia EP - 196 SP - 189 VL - 50 DO - 10.2298/APT1950189P UR - conv_1023 ER -
@article{ author = "Pantović-Spajić, Katarina and Sakan, S. and Đorđević, D. and Šoštarić, Tatjana and Lopičić, Zorica and Janićijević, A. and Stojanović, Ksenija", year = "2019", abstract = "The purpose of this paper was to investigate the effectiveness of three different extraction agents for the extraction of 25 elements from sediment samples collected from 4 artificial lakes and 12 rivers in Serbia (33 samples in total). The extraction efficiency of the agents was evaluated by its ability to extract the highest quantity of the elements. For that purpose, three acids (1M HCl, 2M HNO3 and 0.43M CH3COOH) have been used. Inductively coupled plasma atomic emission spectrometry (ICP-OES) was used for quantitative determination of following elements: Al, As, B, Ba, Be, Bi, Ca, Cd, Cr, Co, Cu, Fe, Hg, K, Li, Mg, Mn, Ni, Na, Pb, Sb, Se, Sr, V, and Zn. The extraction with 1M HCl has shown the best results for the majority of investigated elements (especially Sr, Mn and Ca). Antimony (Sb) was detected only after extraction with 0.43M CH3COOOH, while selenium (Se) could not be detected when 2M HNO3 was applied as extraction agents. The present study could be very useful for choosing a suitable method for specific elements and also can be helpful in the evaluation of the contaminants in freshwater sediments in Serbia. This might contribute to environmental risk assessment of the present elements.", publisher = "Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad", journal = "Acta Periodica Technologica", title = "Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia", pages = "196-189", volume = "50", doi = "10.2298/APT1950189P", url = "conv_1023" }
Pantović-Spajić, K., Sakan, S., Đorđević, D., Šoštarić, T., Lopičić, Z., Janićijević, A.,& Stojanović, K.. (2019). Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia. in Acta Periodica Technologica Univerzitet u Novom Sadu - Tehnološki fakultet, Novi Sad., 50, 189-196. https://doi.org/10.2298/APT1950189P conv_1023
Pantović-Spajić K, Sakan S, Đorđević D, Šoštarić T, Lopičić Z, Janićijević A, Stojanović K. Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia. in Acta Periodica Technologica. 2019;50:189-196. doi:10.2298/APT1950189P conv_1023 .
Pantović-Spajić, Katarina, Sakan, S., Đorđević, D., Šoštarić, Tatjana, Lopičić, Zorica, Janićijević, A., Stojanović, Ksenija, "Comparison of extraction agents for metal determination in sediments from artificial lakes and rivers in Serbia" in Acta Periodica Technologica, 50 (2019):189-196, https://doi.org/10.2298/APT1950189P ., conv_1023 .