Synthesis of Highly Porous Al2O3-YAG Composite Ceramics
Апстракт
Al2O3-YAG composite was obtained by sintering of porous Al2O3 preforms infiltrated with water solution of aluminium nitrate nonahydrate, Al(NO3)(3)center dot 9H(2)O and yttrium nitrate hexahydrate, Y(NO3)(3)center dot 6H(2)O. Al2O3 preforms with porosity varying from 26 to 50% were obtained after sintering at temperature ranging from 1100 to 1500 degrees C. Sintering of the infiltrated Al2O3 preforms led to formation of YAG particles due to reaction between Y2O3 and Al2O3 at high temperature. It was found that variation of porosity of alumina preforms and sintering temperature is an effective way to fabricate Al2O3-YAG composite with an unusual combination of properties. Open porosity was in the range 15-35%, specific surface was 0.6-6.1 m(2)/g, pore size was 150-900 nm whereas compressive strength was from 50 to 250 MPa. The effect of sintering temperature on YAG formation and phase composition were investigated using X-ray diffractometry whereas microstructure of the composite was an...alysed by scanning electron microscopy.
Кључне речи:
Porous ceramics / Composites / Al2O3-YAGИзвор:
Science of Sintering, 2016, 48, 3, 303-315Издавач:
- Međunarodni Institut za nauku o sinterovanju, Beograd
Финансирање / пројекти:
DOI: 10.2298/SOS1603303E
ISSN: 0350-820X
WoS: 000393312300004
Scopus: 2-s2.0-85012255186
Институција/група
Institut za tehnologiju nuklearnih i drugih mineralnih sirovinaTY - JOUR AU - Egelja, Adela AU - Majstorović, Jelena AU - Vuković, Nikola AU - Stanković, Miroslav AU - Bucevac, Dušan PY - 2016 UR - https://ritnms.itnms.ac.rs/handle/123456789/406 AB - Al2O3-YAG composite was obtained by sintering of porous Al2O3 preforms infiltrated with water solution of aluminium nitrate nonahydrate, Al(NO3)(3)center dot 9H(2)O and yttrium nitrate hexahydrate, Y(NO3)(3)center dot 6H(2)O. Al2O3 preforms with porosity varying from 26 to 50% were obtained after sintering at temperature ranging from 1100 to 1500 degrees C. Sintering of the infiltrated Al2O3 preforms led to formation of YAG particles due to reaction between Y2O3 and Al2O3 at high temperature. It was found that variation of porosity of alumina preforms and sintering temperature is an effective way to fabricate Al2O3-YAG composite with an unusual combination of properties. Open porosity was in the range 15-35%, specific surface was 0.6-6.1 m(2)/g, pore size was 150-900 nm whereas compressive strength was from 50 to 250 MPa. The effect of sintering temperature on YAG formation and phase composition were investigated using X-ray diffractometry whereas microstructure of the composite was analysed by scanning electron microscopy. PB - Međunarodni Institut za nauku o sinterovanju, Beograd T2 - Science of Sintering T1 - Synthesis of Highly Porous Al2O3-YAG Composite Ceramics EP - 315 IS - 3 SP - 303 VL - 48 DO - 10.2298/SOS1603303E UR - conv_786 ER -
@article{ author = "Egelja, Adela and Majstorović, Jelena and Vuković, Nikola and Stanković, Miroslav and Bucevac, Dušan", year = "2016", abstract = "Al2O3-YAG composite was obtained by sintering of porous Al2O3 preforms infiltrated with water solution of aluminium nitrate nonahydrate, Al(NO3)(3)center dot 9H(2)O and yttrium nitrate hexahydrate, Y(NO3)(3)center dot 6H(2)O. Al2O3 preforms with porosity varying from 26 to 50% were obtained after sintering at temperature ranging from 1100 to 1500 degrees C. Sintering of the infiltrated Al2O3 preforms led to formation of YAG particles due to reaction between Y2O3 and Al2O3 at high temperature. It was found that variation of porosity of alumina preforms and sintering temperature is an effective way to fabricate Al2O3-YAG composite with an unusual combination of properties. Open porosity was in the range 15-35%, specific surface was 0.6-6.1 m(2)/g, pore size was 150-900 nm whereas compressive strength was from 50 to 250 MPa. The effect of sintering temperature on YAG formation and phase composition were investigated using X-ray diffractometry whereas microstructure of the composite was analysed by scanning electron microscopy.", publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd", journal = "Science of Sintering", title = "Synthesis of Highly Porous Al2O3-YAG Composite Ceramics", pages = "315-303", number = "3", volume = "48", doi = "10.2298/SOS1603303E", url = "conv_786" }
Egelja, A., Majstorović, J., Vuković, N., Stanković, M.,& Bucevac, D.. (2016). Synthesis of Highly Porous Al2O3-YAG Composite Ceramics. in Science of Sintering Međunarodni Institut za nauku o sinterovanju, Beograd., 48(3), 303-315. https://doi.org/10.2298/SOS1603303E conv_786
Egelja A, Majstorović J, Vuković N, Stanković M, Bucevac D. Synthesis of Highly Porous Al2O3-YAG Composite Ceramics. in Science of Sintering. 2016;48(3):303-315. doi:10.2298/SOS1603303E conv_786 .
Egelja, Adela, Majstorović, Jelena, Vuković, Nikola, Stanković, Miroslav, Bucevac, Dušan, "Synthesis of Highly Porous Al2O3-YAG Composite Ceramics" in Science of Sintering, 48, no. 3 (2016):303-315, https://doi.org/10.2298/SOS1603303E ., conv_786 .