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Synthesis of Highly Porous Al2O3-YAG Composite Ceramics

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2016
403.pdf (1.878Mb)
Authors
Egelja, Adela
Majstorović, Jelena
Vuković, Nikola
Stanković, Miroslav
Bucevac, Dušan
Article (Published version)
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Abstract
Al2O3-YAG composite was obtained by sintering of porous Al2O3 preforms infiltrated with water solution of aluminium nitrate nonahydrate, Al(NO3)(3)center dot 9H(2)O and yttrium nitrate hexahydrate, Y(NO3)(3)center dot 6H(2)O. Al2O3 preforms with porosity varying from 26 to 50% were obtained after sintering at temperature ranging from 1100 to 1500 degrees C. Sintering of the infiltrated Al2O3 preforms led to formation of YAG particles due to reaction between Y2O3 and Al2O3 at high temperature. It was found that variation of porosity of alumina preforms and sintering temperature is an effective way to fabricate Al2O3-YAG composite with an unusual combination of properties. Open porosity was in the range 15-35%, specific surface was 0.6-6.1 m(2)/g, pore size was 150-900 nm whereas compressive strength was from 50 to 250 MPa. The effect of sintering temperature on YAG formation and phase composition were investigated using X-ray diffractometry whereas microstructure of the composite was an...alysed by scanning electron microscopy.

Keywords:
Porous ceramics / Composites / Al2O3-YAG
Source:
Science of Sintering, 2016, 48, 3, 303-315
Publisher:
  • Međunarodni Institut za nauku o sinterovanju, Beograd
Funding / projects:
  • Synthesis, processing and characterization of nanostructured materials for application in the field of energy, mechanical engineering, environmental protection and biomedicine (RS-45012)

DOI: 10.2298/SOS1603303E

ISSN: 0350-820X

WoS: 000393312300004

Scopus: 2-s2.0-85012255186
[ Google Scholar ]
6
5
URI
https://ritnms.itnms.ac.rs/handle/123456789/406
Collections
  • Radovi istraživača / Researchers’ publications
Institution/Community
Institut za tehnologiju nuklearnih i drugih mineralnih sirovina
TY  - JOUR
AU  - Egelja, Adela
AU  - Majstorović, Jelena
AU  - Vuković, Nikola
AU  - Stanković, Miroslav
AU  - Bucevac, Dušan
PY  - 2016
UR  - https://ritnms.itnms.ac.rs/handle/123456789/406
AB  - Al2O3-YAG composite was obtained by sintering of porous Al2O3 preforms infiltrated with water solution of aluminium nitrate nonahydrate, Al(NO3)(3)center dot 9H(2)O and yttrium nitrate hexahydrate, Y(NO3)(3)center dot 6H(2)O. Al2O3 preforms with porosity varying from 26 to 50% were obtained after sintering at temperature ranging from 1100 to 1500 degrees C. Sintering of the infiltrated Al2O3 preforms led to formation of YAG particles due to reaction between Y2O3 and Al2O3 at high temperature. It was found that variation of porosity of alumina preforms and sintering temperature is an effective way to fabricate Al2O3-YAG composite with an unusual combination of properties. Open porosity was in the range 15-35%, specific surface was 0.6-6.1 m(2)/g, pore size was 150-900 nm whereas compressive strength was from 50 to 250 MPa. The effect of sintering temperature on YAG formation and phase composition were investigated using X-ray diffractometry whereas microstructure of the composite was analysed by scanning electron microscopy.
PB  - Međunarodni Institut za nauku o sinterovanju, Beograd
T2  - Science of Sintering
T1  - Synthesis of Highly Porous Al2O3-YAG Composite Ceramics
EP  - 315
IS  - 3
SP  - 303
VL  - 48
DO  - 10.2298/SOS1603303E
UR  - conv_786
ER  - 
@article{
author = "Egelja, Adela and Majstorović, Jelena and Vuković, Nikola and Stanković, Miroslav and Bucevac, Dušan",
year = "2016",
abstract = "Al2O3-YAG composite was obtained by sintering of porous Al2O3 preforms infiltrated with water solution of aluminium nitrate nonahydrate, Al(NO3)(3)center dot 9H(2)O and yttrium nitrate hexahydrate, Y(NO3)(3)center dot 6H(2)O. Al2O3 preforms with porosity varying from 26 to 50% were obtained after sintering at temperature ranging from 1100 to 1500 degrees C. Sintering of the infiltrated Al2O3 preforms led to formation of YAG particles due to reaction between Y2O3 and Al2O3 at high temperature. It was found that variation of porosity of alumina preforms and sintering temperature is an effective way to fabricate Al2O3-YAG composite with an unusual combination of properties. Open porosity was in the range 15-35%, specific surface was 0.6-6.1 m(2)/g, pore size was 150-900 nm whereas compressive strength was from 50 to 250 MPa. The effect of sintering temperature on YAG formation and phase composition were investigated using X-ray diffractometry whereas microstructure of the composite was analysed by scanning electron microscopy.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Synthesis of Highly Porous Al2O3-YAG Composite Ceramics",
pages = "315-303",
number = "3",
volume = "48",
doi = "10.2298/SOS1603303E",
url = "conv_786"
}
Egelja, A., Majstorović, J., Vuković, N., Stanković, M.,& Bucevac, D.. (2016). Synthesis of Highly Porous Al2O3-YAG Composite Ceramics. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 48(3), 303-315.
https://doi.org/10.2298/SOS1603303E
conv_786
Egelja A, Majstorović J, Vuković N, Stanković M, Bucevac D. Synthesis of Highly Porous Al2O3-YAG Composite Ceramics. in Science of Sintering. 2016;48(3):303-315.
doi:10.2298/SOS1603303E
conv_786 .
Egelja, Adela, Majstorović, Jelena, Vuković, Nikola, Stanković, Miroslav, Bucevac, Dušan, "Synthesis of Highly Porous Al2O3-YAG Composite Ceramics" in Science of Sintering, 48, no. 3 (2016):303-315,
https://doi.org/10.2298/SOS1603303E .,
conv_786 .

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