European Regional Development Fund through CEITEC-Central European Institute of Technology [CZ.1.05/1.1.00/02.0068]

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European Regional Development Fund through CEITEC-Central European Institute of Technology [CZ.1.05/1.1.00/02.0068]

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Publications

Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol

Ćosović, Aleksandar; Zak, Tomas; Glišić, Sandra B.; Sokić, Miroslav; Lazarević, Slavica; Ćosović, Vladan; Orlović, Aleksandar M.

(Elsevier Science Bv, Amsterdam, 2016)

TY  - JOUR
AU  - Ćosović, Aleksandar
AU  - Zak, Tomas
AU  - Glišić, Sandra B.
AU  - Sokić, Miroslav
AU  - Lazarević, Slavica
AU  - Ćosović, Vladan
AU  - Orlović, Aleksandar M.
PY  - 2016
UR  - https://ritnms.itnms.ac.rs/handle/123456789/389
AB  - Nano-crystalline nickel ferrite has a broad range of applications due to its favourable magnetic properties. Those characteristics can be significantly influenced by the synthesis pathway including methods conducted in the presence of supercritical alcohols. Nano-crystalline NiFe2O4 powders were obtained in the reaction under subcritical and supercritical conditions of ethanol. Both high pressure synthesis routes resulted in powders with smaller primary particles and higher mesoporosity than co-precipitation method. Upon the annealing treatment the average crystallite size increased while material structure remained uniform, resulting in significantly enhanced magnetic properties, such as coercivity and remanence. It was found that synthesis under supercritical conditions provides higher conversion but also material with larger average crystallite size upon annealing. The time and temperature of annealing stage significantly influenced the morphology and magnetic properties of the obtained powders.
PB  - Elsevier Science Bv, Amsterdam
T2  - Journal of Supercritical Fluids
T1  - Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol
EP  - 105
SP  - 96
VL  - 113
DO  - 10.1016/j.supflu.2016.03.014
UR  - conv_759
ER  - 
@article{
author = "Ćosović, Aleksandar and Zak, Tomas and Glišić, Sandra B. and Sokić, Miroslav and Lazarević, Slavica and Ćosović, Vladan and Orlović, Aleksandar M.",
year = "2016",
abstract = "Nano-crystalline nickel ferrite has a broad range of applications due to its favourable magnetic properties. Those characteristics can be significantly influenced by the synthesis pathway including methods conducted in the presence of supercritical alcohols. Nano-crystalline NiFe2O4 powders were obtained in the reaction under subcritical and supercritical conditions of ethanol. Both high pressure synthesis routes resulted in powders with smaller primary particles and higher mesoporosity than co-precipitation method. Upon the annealing treatment the average crystallite size increased while material structure remained uniform, resulting in significantly enhanced magnetic properties, such as coercivity and remanence. It was found that synthesis under supercritical conditions provides higher conversion but also material with larger average crystallite size upon annealing. The time and temperature of annealing stage significantly influenced the morphology and magnetic properties of the obtained powders.",
publisher = "Elsevier Science Bv, Amsterdam",
journal = "Journal of Supercritical Fluids",
title = "Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol",
pages = "105-96",
volume = "113",
doi = "10.1016/j.supflu.2016.03.014",
url = "conv_759"
}
Ćosović, A., Zak, T., Glišić, S. B., Sokić, M., Lazarević, S., Ćosović, V.,& Orlović, A. M.. (2016). Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol. in Journal of Supercritical Fluids
Elsevier Science Bv, Amsterdam., 113, 96-105.
https://doi.org/10.1016/j.supflu.2016.03.014
conv_759
Ćosović A, Zak T, Glišić SB, Sokić M, Lazarević S, Ćosović V, Orlović AM. Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol. in Journal of Supercritical Fluids. 2016;113:96-105.
doi:10.1016/j.supflu.2016.03.014
conv_759 .
Ćosović, Aleksandar, Zak, Tomas, Glišić, Sandra B., Sokić, Miroslav, Lazarević, Slavica, Ćosović, Vladan, Orlović, Aleksandar M., "Synthesis of nano-crystalline NiFe2O4 powders in subcritical and supercritical ethanol" in Journal of Supercritical Fluids, 113 (2016):96-105,
https://doi.org/10.1016/j.supflu.2016.03.014 .,
conv_759 .
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