X-Ray diffraction analysis of mechanically activated natural zeolite
2022
Аутори
Đorđević, NatašaStojanović, Jovica
Grubišić, Mirko
Mihajlović, Slavica
Остала ауторства
Obradović, NinaMančić, Lidija
Конференцијски прилог (Објављена верзија)
Метаподаци
Приказ свих података о документуАпстракт
In this research, preliminary investigations of the influence of mechanical energy during the
milling process on a sample of natural zeolite were performed. Activation was performed in a
mill with a ceramic vessel and ceramic balls for 15, 30 and 60 minutes. The XRD method was
used to determine the phase composition. The XRD patterns were obtained on a Philips PW-
1710 automated diffractometer using a Cu tube operated at 40 kV and 30 mA. All the XRD
measurements were performed at room temperature in a stationary sample holder. Crystallite
domain size were calcuclated using SiroQuant v4 software. The mineral composition of the analyzed sample is as follows: clinoptilolite-heulandite zeolite types, smectite/chlorite
minerals, quartz, feldspars, mica, and irregularly interstratified clay minerals. Crystallinity
degree of all present phases decreases with activation time in comparison to the non-activated
sample. Crystallite domain size for diffration maximum (020) of non-activate...d sample was
533 Å (FWHM 0.240 o), and decreases with acitivation time to 202 Å (FWHM 0.275 o) for
sample activated 60 min.
Извор:
10th Serbian Ceramic Society Conference „Advanced Ceramics and Application“, 2022, 78-79Издавач:
- Belgrade : Serbian Ceramic Society
Финансирање / пројекти:
- Министарство науке, технолошког развоја и иновација Републике Србије, институционално финансирање - 200023 (Институт за технологију нуклеарних и других минералних сировина - ИТНМС, Београд) (RS-MESTD-inst-2020-200023)
Институција/група
Institut za tehnologiju nuklearnih i drugih mineralnih sirovinaTY - CONF AU - Đorđević, Nataša AU - Stojanović, Jovica AU - Grubišić, Mirko AU - Mihajlović, Slavica PY - 2022 UR - https://ritnms.itnms.ac.rs/handle/123456789/1130 AB - In this research, preliminary investigations of the influence of mechanical energy during the milling process on a sample of natural zeolite were performed. Activation was performed in a mill with a ceramic vessel and ceramic balls for 15, 30 and 60 minutes. The XRD method was used to determine the phase composition. The XRD patterns were obtained on a Philips PW- 1710 automated diffractometer using a Cu tube operated at 40 kV and 30 mA. All the XRD measurements were performed at room temperature in a stationary sample holder. Crystallite domain size were calcuclated using SiroQuant v4 software. The mineral composition of the analyzed sample is as follows: clinoptilolite-heulandite zeolite types, smectite/chlorite minerals, quartz, feldspars, mica, and irregularly interstratified clay minerals. Crystallinity degree of all present phases decreases with activation time in comparison to the non-activated sample. Crystallite domain size for diffration maximum (020) of non-activated sample was 533 Å (FWHM 0.240 o), and decreases with acitivation time to 202 Å (FWHM 0.275 o) for sample activated 60 min. PB - Belgrade : Serbian Ceramic Society C3 - 10th Serbian Ceramic Society Conference „Advanced Ceramics and Application“ T1 - X-Ray diffraction analysis of mechanically activated natural zeolite EP - 79 SP - 78 ER -
@conference{ author = "Đorđević, Nataša and Stojanović, Jovica and Grubišić, Mirko and Mihajlović, Slavica", year = "2022", abstract = "In this research, preliminary investigations of the influence of mechanical energy during the milling process on a sample of natural zeolite were performed. Activation was performed in a mill with a ceramic vessel and ceramic balls for 15, 30 and 60 minutes. The XRD method was used to determine the phase composition. The XRD patterns were obtained on a Philips PW- 1710 automated diffractometer using a Cu tube operated at 40 kV and 30 mA. All the XRD measurements were performed at room temperature in a stationary sample holder. Crystallite domain size were calcuclated using SiroQuant v4 software. The mineral composition of the analyzed sample is as follows: clinoptilolite-heulandite zeolite types, smectite/chlorite minerals, quartz, feldspars, mica, and irregularly interstratified clay minerals. Crystallinity degree of all present phases decreases with activation time in comparison to the non-activated sample. Crystallite domain size for diffration maximum (020) of non-activated sample was 533 Å (FWHM 0.240 o), and decreases with acitivation time to 202 Å (FWHM 0.275 o) for sample activated 60 min.", publisher = "Belgrade : Serbian Ceramic Society", journal = "10th Serbian Ceramic Society Conference „Advanced Ceramics and Application“", title = "X-Ray diffraction analysis of mechanically activated natural zeolite", pages = "79-78" }
Đorđević, N., Stojanović, J., Grubišić, M.,& Mihajlović, S.. (2022). X-Ray diffraction analysis of mechanically activated natural zeolite. in 10th Serbian Ceramic Society Conference „Advanced Ceramics and Application“ Belgrade : Serbian Ceramic Society., 78-79.
Đorđević N, Stojanović J, Grubišić M, Mihajlović S. X-Ray diffraction analysis of mechanically activated natural zeolite. in 10th Serbian Ceramic Society Conference „Advanced Ceramics and Application“. 2022;:78-79..
Đorđević, Nataša, Stojanović, Jovica, Grubišić, Mirko, Mihajlović, Slavica, "X-Ray diffraction analysis of mechanically activated natural zeolite" in 10th Serbian Ceramic Society Conference „Advanced Ceramics and Application“ (2022):78-79.